dc.contributor.author | Walęcka-Kurczyk, A. | |
dc.contributor.author | Adamek, J. | |
dc.contributor.author | Walczak, K. | |
dc.contributor.author | Michalak, M. | |
dc.contributor.author | Październiok-Holewa, A. | |
dc.date.accessioned | 2022-06-22T11:52:36Z | |
dc.date.available | 2022-06-22T11:52:36Z | |
dc.date.issued | 2022-01-12 | |
dc.identifier.citation | RSC Adv., 2022, 12, 2107. https://doi.org/10.1039/D1RA08124A | en |
dc.identifier.issn | 2046-2069 | |
dc.identifier.other | 10.1039/D1RA08124A | |
dc.identifier.uri | https://depot.ceon.pl/handle/123456789/21363 | |
dc.description.abstract | Here, we report a standardized method for the synthesis of N-protected (1-methoxyalkyl)amines by the electrochemical decarboxylative α-methoxylation of α-amino acid derivatives using the commercially available, easy-to-use, compact ElectraSyn 2.0 setup. The use of equipment with a standardized power source, electrodes, and other accessories allows this experimental procedure to be easily transferred to any laboratory in the world. A simple workup and chromatography-free purification produced the products in excellent yields above 90%. | en |
dc.description.sponsorship | Silesian University of Technology (Poland) Grant BK No. 04/020/BK_22/1035 | |
dc.language.iso | en | |
dc.publisher | Royal Society of Chemistry | en |
dc.rights | Creative Commons Uznanie autorstwa - Użycie niekomercyjne 3.0 | * |
dc.rights.uri | http://creativecommons.org/licenses/by-nc/3.0/pl/legalcode | * |
dc.title | Non-Kolbe electrolysis of N-protected-α-amino acids: a standardized method for the synthesis of N-protected (1-methoxyalkyl)amines | en |
dc.type | article | en |
dc.contributor.organization | Department of Organic Chemistry, Bioorganic Chemistry and Biotechnology, Silesian University of Technology | en |
dc.contributor.organization | Biotechnology Center of Silesian University of Technology | en |
dc.contributor.organization | Institute of Organic Chemistry, Polish Academy of Sciences | en |